TABLE 2.
Summed fractional labelings obtained with the reference strain in continuous cultivations at dilution rate of 0.1 h−1 for different acetate fractionsa
Compound analyzed | Mol wt of unlabeled isotopomer | Biosynthetic precursor(s) | C atoms from biosynthetic precursor(s) present in fragment | Sum of fractional labelings (%) of C atoms in a fragment with the following acetate fraction (C-mol/C-mol of substrate) and labeled substrate used:
|
|||
---|---|---|---|---|---|---|---|
0b [1-13C]glucose | 0.04, [1,2-13C]acetate | 0.46c, [1,2-13C]acetate | 0.90d, [13C6]glucose | ||||
Glc | 331 | Glc 6P | 1, 2, 3, 4, 5, 6 | 91.0 | 6.9 | 277.9 | |
Gly | 175e | 3-PG | 1, 2 | 5.9 | 3.2 | 10.2 | 21.3 |
144f | 3-PG | 1, 2 | 6.2 | 3.1 | 11.4 | ||
85f | 3-PG | 2 | 3.7 | 1.3 | 5.1 | 9.6 | |
Ser | 175e | 3-PG | 1, 2 | 3.1 | 3.1 | 5.9 | 34.0 |
132e | 3-PG | 2, 3 | 33.8 | 2.4 | 5.6 | 31.5 | |
Phe | 143f | PEP | 1, 2 | 3.0 | 2.2 | 4.3 | 25.3 |
192e | PEP + E4P | 2, 2, 3, 3 + 1, 2, 3, 4 | 90.6 | 9.4 | 14.9 | 212.1 | |
Ala | 116e | Pyr | 2, 3 | 36.0 | 3.0 | 12.5 | 14.9 |
99f | Pyr | 2, 3 | 36.0 | 3.2 | 12.5 | 15.1 | |
158f | Pyr | 1, 2, 3 | 38.5 | 4.7 | 18.3 | 21.1 | |
Val | 144e | Pyr | 2, 2, 3, 3 | 73.3 | 6.5 | 27.3 | 21.2 |
143f | Pyr | 1, 2 | 6.9 | 2.9 | 13.8 | 10.2 | |
127f | Pyr | 2, 2, 3, 3 | 73.1 | 6.3 | 26.8 | 20.1 | |
186f | Pyr | 1, 2, 2, 3, 3 | 74.9 | 7.9 | 33.3 | 26.5 | |
Leu | 158e | Pyr + AcCoA | 2, 2, 3, 3 + 2 | 106.1 | 15.6 | 42.3 | 19.8 |
Asp | 188e | OAA | 2, 3, 4 | 57.1 | 11.4 | 39.8 | 7.2 |
115f | OAA | 2 | 12.0 | 3.4 | 11.7 | 2.5 | |
216f | OAA | 1, 2, 3, 4 | 64.4 | 14.3 | 52.8 | 10.0 | |
Thr | 175e | OAA | 1, 2 | 17.8 | 6.8 | 25.0 | 5.0 |
146e | OAA | 2, 3, 4 | 54.5 | 12.1 | 35.7 | 8.2 | |
Ile | 158e | OAA + Pyr | 2, 3, 4 + 2, 3 | 93.7 | 14.5 | 53.4 | 16.9 |
Pro | 142e | α-KG | 2, 3, 4, 5 | 85.5 | 18.8 | 58.3 | 6.9 |
Glu | 143f | α-KG | 1, 2 | 39.9 | 10.5 | 28.4 | 6.5 |
230f | α-KG | 1, 2, 3, 4, 5 | 100.1 | 23.7 | 72.1 | 11.6 | |
Lys | 156e | α-KG + AcCoA | 2, 3, 4, 5 + 2 | 117.2 | 48.5 | 75.6 | 8.4 |
A naturally labeled fragment with n carbon atoms will be labeled n.n%. The biosynthetic precursors indicated are for growth on glucose and ammonia; for some amino acids, the biosynthetic pathways may change for growth on acetate. Abbreviations: 3-PG, 3-phosphoglycerate; Pyr, pyruvate; AcCoA, acetyl-CoA; OAA, oxaloacetate; α-KG, α-ketoglutarate; PEP, phosphoenolpyruvate; E4P, erythrose-4-phosphate; Glc, glucose; Glc 6P, glucose-6-phosphate.
Data are from reference 15.
Only 20% of the acetate fed to the culture was [1,2-13C] acetate.
pH6.
Amino acid analyzed as N-ethoxycarbonyl amino acid ethylester.
Amino acid analyzed as N-(N,N-dimethylaminomethylene) amino acid methylester.