Table 1. X-ray diffraction data.
| Data set* | Native | Rpb4/7 SeMet |
|---|---|---|
| Unit cell axis,† Å | 220.4, 391.4, 282.2 | 223.0, 394.5, 284.4 |
| Wavelength, Å | 0.9185 | 0.9795 (Se peak) |
| Resolution, Å (highest shell) | 50-4.2 (4.35-4.2) | 50-6.5 (6.7-6.5) |
| Unique reflections (highest shell) | 83,431 (7,893) | 25,009 (2,452) |
| Completeness, % (highest shell) | 93.8 (89.5) | 99.9 (100.0) |
| Redundancy | 2.9 | 13.4 |
| I/σI | 6.5 | 9.4 |
| Rsym, % (highest shell) | 9.3 (36.3) | 7.5 (25.8) |
| No. of peaks in anomalous Fourier | - | 13 (5 Se, 8 Zn) |
SeMet, selenomethionine.
*
Diffraction data were collected at the Swiss Light Source.
†
Space group C2221.