TABLE 1.
Data collection and refinement statistics
Values in parentheses are for the highest resolution shell (1.97-1.9 Å).
| FHF2A | |
|---|---|
| Data collection | |
| Space group | P21 |
| Cell dimensions, a, b, c (Å); β (°) | 52.218, 57.998, 52.236; 93.791 |
| Resolution (Å) | 50.0-1.9 |
| Rsym (%) | 4.4 (20.2) |
| I/σI | 34.9 |
| Completeness (%) | 94.8 (86.8) |
| Redundancy | 8.2 (7.4) |
| Refinement | |
| Resolution (Å) | 25.0-1.9 |
| No. reflections | 23,092 |
| Rcryst/Rfree (%)a | 21.9/25.1 |
| No. atoms | |
| Protein | 2,360 |
| Water | 130 |
| B-Factors | |
| Protein | 25.5 |
| Water | 30.6 |
| Root mean square deviations | |
| Bond lengths (Å) | 0.006 |
| Bond angles (°) | 1.4 |
a 10% of the reflections were used for calculation of Rfree.