Table 3.
Native Disulfide-Linked Peptides in Digest of RNaseA under Basic and Acidic Conditions Identified in the Confirmatory Searcha
digestion condition | disulfide bond | number of matches | pp value sum/high | disulfide-linked peptides |
---|---|---|---|---|
pH = 8.0 | C26—C84 | 41 | 554.9/21.9 | [26–29]-S-S-[80–85] |
[26–30]-S-S-[80–85] | ||||
[26–31]-S-S-[80–85] | ||||
[26–31]-S-S-[77–85] | ||||
C40—C95 | 74 | 629.3/18.9 | [40–46]-S-S-[93–97] | |
[40–46]-S-S-[92–97] | ||||
[40–46]-S-S-[92–98] | ||||
C58—C110 | 10 | 112.7/17.2 | [47–61]-S-S-[105–115] | |
C65—C72 | 58 | 807.6/32.9 | [62–73]* | |
[62–76]* | ||||
[62–66]-S-S-[67–73] | ||||
[62–66]-S-S-[67–76] | ||||
pH = 6.0 | C26—C84 | 31 | 431.6/20.5 | [26–29]-S-S-[80–85] |
[26–30]-S-S-[80–85] | ||||
[26–31]-S-S-[80–85] | ||||
C40—C95 | 46 | 386.4/15.4 | [40–46]-S-S-[93–97] | |
[40–46]-S-S-[92–97] | ||||
[40–46]-S-S-[92–98] | ||||
[38–46]-S-S-[92–97] | ||||
C58—C110 | 11 | 129.8/17.5 | [52–61]-S-S-[105–115] | |
[47–61]-S-S-[105–115] | ||||
C65—C72 | 6 | 79.3/21.9 | [62–73]* | |
[62–66]-S-S-[67–73] | ||||
[62–66]-S-S-[67–76] |
Asterisk (*): peptides with intrachain disulfide bond.