Table 1.
Data Collection and Refinement Statistics
| Data Collection | |
|---|---|
| Space group | P6522 |
| Cell dimensions | |
| a, b, c (Å) | 134.3, 134.3, 428.1 |
| α, β, γ (°) | 90, 90, 120 |
| Resolution (Å) | 3.3 (3.5–3.3) |
| Rsym or Rmerge | 0.099 (0.674) |
| I / σI | 10.4 (1.9) |
| Completeness (%) | 98.9 (99.9) |
| Redundancy | 5.2 (5.4) |
| Refinement | |
| Resolution (Å) | 44–3.3 (3.4–3.3) |
| No. reflections | 34250 (2651) |
| Rwork/Rfree | 0.24/0.3 (0.26/0.3) |
| No. atoms | 9848 |
| Protein | 9813 |
| Ligand/ion | 35 |
| Water | 0 |
| B factors | 129 |
| Protein | 129 |
| Ligand/ion | 97 |
| Water | 0 |
| Rmsds | |
| Bond lengths (Å) | 0.01 |
| Bond angles (°) | 1.33 |
The numbers in parentheses refer to statistics for the highest-resolution bin.